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Vibrio cholearae  presence of toxigenic 01 or non-01Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 9. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Vibrio parahaemolyticus10000/glevel ³ (Kanagawa positive or negative)Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 9. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Vibrio vulnificus  presence of pathogenic organismBacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 9. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Annatto extract  GMPIn-house validated method 21 CFR Section73.302,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual Investigations Operations Manual
Dehydrated beets (beet powder)  GMPIn-house validated method 21 CFR Section73.403,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual Investigations Operations Manual
Canthaxanthin30mg/lbof solid or semisolid food or per pint of liquid foodOFFICIAL ANALYTICAL PROTOCOL p. 20 21 CFR Section73.754,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.fda.gov/ohrms/dockets/dockets/95s0316/95s-0316-rpt0237-07-Tab-E-vol172.pdf OFFICIAL ANALYTICAL PROTOCOL p. 20 Investigations Operations Manual Investigations Operations Manual
Caramel  GMPIn-house validated method 21 CFR Section73.855,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual Investigations Operations Manual
Riboflavin  GMPAOAC 970.65 21 CFR Section73.45022,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Saffron  GMPAcceptability determination 21 CFR Section73.50023,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Titanium dioxide1%by wt. of foodIn-house validated method 21 CFR Section73.57524,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Tomato lycopene extract; tomato lycopene concentrate  GMPAcceptability determination 21 CFR Section73.58525,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Fluoride150ppm ICP/MS Food and Drug Regulation,Devertion 15 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocum FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p156-157 FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p125-126
Methyl mercury:1ppm Methods for the Determination of Metals in Environmental Samples No.200.2, 200.3, 245.1,245.3, 245.5, 245.6 Sec 540.600 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen http://www.epa.gov/nerlcwww/methmans.html Guidance for Assessing Chemical Contaminant Data for Use in Fish Advisories Volume 1 Fish Sampling and AnalysisThird Edition, Charpter6
Paralytic shellfish poison:0.8ppm(80m g/100 g)saxitoxin equivalentParalytic Shellfish Poison (PSP) and Neurotoxic Shellfish Poison (NSP) Methods, Recommended Procedures for the Examination of Sea Water and Shellfish, 4th Edition Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Se http://www.issc.org/client_resources/2007%20nssp%20guide/section%20iv%20chap%20ii%20.10.pdf Guidance for Assessing Chemical Contaminant Data for Use in Fish Advisories Volume 1 Fish Sampling and AnalysisThird Edition, Charpter6
Mirex:0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 304) Sec 575.100 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen Pesticide Analytical Manual (PAM)Vol. I (section 102)
Chlordecone:0.3ppm Pesticide Analytical Manual (PAM) vol.I (section 304) Sec 575.100 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen Pesticide Analytical Manual (PAM)Vol. I (section 102)
Aldrin and dieldrin:0.3ppm Pesticide Analytical Manual (PAM) vol.I (section 304) Sec 575.100 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen Pesticide Analytical Manual (PAM)Vol. I (section 102)
SIMAZINE12ppm Pesticide Analytical Manual (PAM) vol.I (section 304) 40 CFR 180.213a (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Seafood/FishandFi Pesticide Analytical Manual (PAM)Vol. I (section 102)
B-Apo-8'-carotenal15mg/lb or mg/pt AOAC 941.15 21 CFR Section73.906,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual Investigations Operations Manual
B-Carotene  GMPAOAC 941.15 21 CFR Section73.957,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Cochineal extract  GMPAcceptability determination 21 CFR Section73.1008,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual Investigations Operations Manual
Toasted partially defatted cooked cottonseed flour  GMPAcceptability determination 21 CFR Section73.1401,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Salmonella species  presence of pathogenic organismBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 5. Compliance Policy Guide Section 555.300 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDoc http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Staphylococcus aureus10000/gpositive for staphylococcal enterotoxin, or level ³ (MPN)Bacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 12. FDA/EPA guidance levels in seafoods (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Clostridium botulinum  Presence of viable spores or vegetative cells in products that will support their growth; or Presence of toxinBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 17. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Turmeric  GMPIn-house validated method 21 CFR Section73.60026,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Turmeric oleoresin  GMPIn-house validated method 21 CFR Section73.61527,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Blue  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.10128Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Blue  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.10229Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Green  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.20330Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Amnesic shellfish poison:20ppmdomoic acid, except in the viscera of Dungeness crab, where 30 ppm is permittedbioassay/HPLC Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Se http://www.fda.gov/Food/FoodSafety/FoodborneIllness/FoodborneIllnessFoodbornePathogensNaturalToxins/BadBugBook/ucm070795.htm Guidance for Assessing Chemical Contaminant Data for Use in Fish Advisories Volume 1 Fish Sampling and AnalysisThird Edition, Charpter6
Histamine500ppmset based on toxicity; 50 ppm set as defect action level, because histamine is generally not uniformly distributed in a decomposed fish; therefore, if 50 ppm is found possibility that other units may exceed 500 ppmFish and Fishery Products Hazards and Controls Guide. 2nd edn.,p 91-92 Compliance Policy Guide Section 540.525 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDo Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1.
Sulfamerazine:  no residue permittedTLC/GC/ESI-MS 21 CFR 556.660 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Seafood/FishandFis 2005 National Residue Program Data - Red Book/Appendix IV FSIS Laboratory Analytical Methods FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p125-126
FLURIDONE0.5ppm Pesticide Analytical Manual (PAM) vol.I (section 304) 40 CFR 180.420 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Seafood/FishandFis Pesticide Analytical Manual (PAM)Vol. I (section 102)
Enterotoxigenic Escherichia coli1000ETEC/gpresence of pathogenic organismBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 4. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Listeria monocytogenes  presence of pathogenic organismBacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 10 and 11. Compliance Programme 7303.842 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Sea http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Paprika oleoresin  GMPIn-house validated method 21 CFR Section73.3452,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Fruit juice  GMPAcceptability determination 21 CFR Section73.25016,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Vegetable juice  GMPAcceptability determination 21 CFR Section73.26017,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Carrot oil  GMPIn-house validated method 21 CFR Section73.30018,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Paprika  GMPIn-house validated method 21 CFR Section73.34019,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Red  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.34034Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Yellow  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.70535Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
FD&C Yellow  GMPAOAC 966.21, AOAC 988.13 21 CFR Section74.70636Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual http://www.fda.gov/ICECI/Inspections/IOM/default.htm
Arsenic3.5ppmGMPICP/MS Food and Drug Regulation,Devertion 15 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocum FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p156-157 FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p125-126
Unsanctioned drugs*:  no residue permittedไม่ระบุ Compliance Policy Guide Section 615.200 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDoc 2005 National Residue Program Data - Red Book/Appendix IV FSIS Laboratory Analytical Methods FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p125-126
Polychlorinated biphenyls:0.2ppm Pesticide Analytical Manual (PAM) vol.I (section 304) 21 CFR 109.30 (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/Seafood/FishandFi Pesticide Analytical Manual (PAM)Vol. I (section 102)
DDT, TDE and DDE:5ppm Pesticide Analytical Manual (PAM) vol.I (section 304) Sec 575.100 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen Pesticide Analytical Manual (PAM)Vol. I (section 102)
Heptachlor and heptachlor epoxide:0.3ppm Pesticide Analytical Manual (PAM) vol.I (section 304) Sec 575.100 Compliance Policy Guide (Fish and Fisheries Products Hazards and Controls Guidance Third Edition,Appendix 5 - FDA & EPA Safety Levels in Regulations and Guidance ; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocumen Pesticide Analytical Manual (PAM)Vol. I (section 102)
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