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Fruit juice  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.25016,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Vegetable juice  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.26017,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Carrot oil  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.30018,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Paprika  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.34019,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
FD&C Blue  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.10229Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
FD&C Green  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.20330Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
FD&C Red  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.34034Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
FD&C Yellow  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.70535Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
d-Phenothrin0.01ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) www.mrldatabase.com Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303)
DIAZINON0.5ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
DIURON0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
DIURON0.4ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Ethoprop (ethoprophos)0.02ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
FENAMIPHOS0.3ppm(No US registrations aqs of Dec. 31, 2009)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Fosetyl-aluminium (Aluminum tris(O-ethylphosphonate))0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Fosetyl-aluminium (Aluminum tris(O-ethylphosphonate))0.1ppm(fodder)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Metalaxyl0.1ppm(fodder)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
O-Phenylphenol and its sodium salt10ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Oxamyl1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Oxamyl2ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Quizalofop-ethyl0.1ppm(Regional registrations)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Spinetoram0.04ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) www.mrldatabase.com Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Spinosad0.02ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Spinosad0.08ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
PARAQUAT0.05ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
PARAQUAT0.25ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Piperonyl Butoxide8ppm(postharvest )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Propiconazole4.5ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
TRIADIMEFON2ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Triflumizole4ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Benzene Hexachloride (BHC)0.05ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Compliance Policy Guide Section 575.100 (Guidance for Industry: Action Levels for Poisonous or Deleterious Substances in Human Food and Animal Feed; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/ChemicalContaminantsandP Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
CHLORDANE0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Compliance Policy Guide Section 575.100 (Guidance for Industry: Action Levels for Poisonous or Deleterious Substances in Human Food and Animal Feed; http://www.fda.gov/Food/GuidanceComplianceRegulatoryInformation/GuidanceDocuments/ChemicalContaminantsand Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102)
FD&C Yellow  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.70636Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Tin250ppm ICP/MS Food and Drug Regulation,Devertion 15 FOOD SAFETY AND INSPECTION SERVICE,National Residue Program Scheduled Sampling Plans,p156-157 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
1-NAPHTHALENEACETIC ACID0.05ppm(from the application of the sodium salt to the growing crop)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM)Vol. I (section 102)
AMETRYN0.05ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Endosulfan1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Endosulfan20ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
EPTC (S-Ethyl dipropylthiocarbamate)0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Ethephon2ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Paprika oleoresin  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.3452,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Riboflavin  Good Manufacturing Practice(GMP)AOAC 970.65 21 CFR Section73.45022,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Saffron  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.50023,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Titanium dioxide≤ 1.0% by wt. of food  In-house validated method 21 CFR Section73.57524,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Fosetyl-aluminium (Aluminum tris(O-ethylphosphonate))0.1ppm(fodder)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Glyphosate0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
HEXAZINONE0.6ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
HYDRAMETHYLNON0.05ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Enterotoxigenic Escherichia coli  ไม่ระบุBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 4. FDA Survey of Imported Fresh produce (FY 2001 assignment)(http://www.fda.gov/Food/FoodSafety/Product-SpecificInformation/FruitsVegetablesJuices/GuidanceComplianceRegulatoryInformation/ucm118887.htm) http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Salmonella species  ไม่ระบุBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 5. FDA Survey of Imported Fresh produce (FY 2001 assignment)(http://www.fda.gov/Food/FoodSafety/Product-SpecificInformation/FruitsVegetablesJuices/GuidanceComplianceRegulatoryInformation/ucm118887.htm) http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Shigella  ไม่ระบุBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 6. FDA Survey of Imported Fresh produce (FY 2001 assignment)(http://www.fda.gov/Food/FoodSafety/Product-SpecificInformation/FruitsVegetablesJuices/GuidanceComplianceRegulatoryInformation/ucm118887.htm) http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm
Clostridium botulinum  ไม่ระบุBacteriological Analytical Manual, 8th Edition, Revision A, 1998. Chapter 17. FDA Survey of Imported Fresh produce (FY 2001 assignment)(http://www.fda.gov/Food/FoodSafety/Product-SpecificInformation/FruitsVegetablesJuices/GuidanceComplianceRegulatoryInformation/ucm118887.htm) http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/BacteriologicalAnalyticalManualBAM/default.htm Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1. Bacteriological Analytical Manual, Edition 8, Revision A, 1998. Chapter 1.
B-Apo-8'-carotenal15mg/lbof solid , 15 mg/pt liquidAOAC 941.15 21 CFR Section73.906,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
B-Carotene  Good Manufacturing Practice(GMP)AOAC 941.15 21 CFR Section73.957,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.codexalimentarius.net/web/standard_list.jsp CXS_234e[1].pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Cochineal extract  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.1008,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Toasted partially defatted cooked cottonseed flour  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.1401,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Tomato lycopene extract; tomato lycopene concentrate  Good Manufacturing Practice(GMP)Acceptability determination 21 CFR Section73.58525,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm UNITED STATES DEPARTMENT OF FOOD SAFETY AND INSPECTION SERVICEAGRICULTURE WASHINGTON, DC,FSIS Directive 7120.1, Amendment 21 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Turmeric  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.60026,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Turmeric oleoresin  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.61527,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
FD&C Blue  Good Manufacturing Practice(GMP)AOAC 966.21, AOAC 988.13 21 CFR Section74.10128Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.eoma.aoac.org/ Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Annatto extract  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.302,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Dehydrated beets (beet powder)  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.403,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Canthaxanthin30mg/lbof solid or semisolid food or per pint of liquid foodOFFICIAL ANALYTICAL PROTOCOL p. 20 21 CFR Section73.754,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm http://www.fda.gov/ohrms/dockets/dockets/95s0316/95s-0316-rpt0237-07-Tab-E-vol172.pdf OFFICIAL ANALYTICAL PROTOCOL p. 20 Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Caramel  Good Manufacturing Practice(GMP)In-house validated method 21 CFR Section73.855,Summary of Color Additives for Use in United States in Foods, Drugs, Cosmetics, and Medical Devices, http://www.fda.gov/ForIndustry/ColorAdditives/ColorAdditiveInventories/ucm115641.htm ftp://ftp.fao.org/codex/ccmas23/ma01_09e.pdf ma01_09e.pdf Investigations Operations Manual, chapter 4 http://www.fda.gov/downloads/ICECI/Inspections/IOM/UCM123507.pdf http://www.fda.gov/ICECI/Inspections/IOM/default.htm Investigations Operations Manual, chapter 4.pdf Investigations Operations Manual, chapter 4.pdf
Benomyl35ppm(postharvest (Expired 1/1/08) )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
BROMACIL0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Carbaryl2ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303)
Cloprop, 3-CPA (2-(m-Chlorophenoxy) propionic acid0.3ppm(Expired 2/1/07)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM) vol.I (section 302-303)
Inorganic bromide residues resulting from fumigation with methylbromide20ppm(postharvest )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Malathion8ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Metalaxyl0.1ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Metalaxyl0.1ppm(fodder)Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Propiconazole7ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Pyrethrins1ppm(postharvest )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Pyriproxyfen0.3ppm Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
Pyriproxyfen1.1ppm(process residue )Pesticide Analytical Manual (PAM) vol.I (section 302-303) Index to Pesticide Chemical Names,Part 180 Tolerance Information, and Food and Feed Commodities (http://www.epa.gov/pesticides/regulating/tolerances-commodity.pdf) Pesticide Analytical Manual (PAM) vol.I (section 302-303) Pesticide Analytical Manual (PAM)Vol. I (section 102) Pesticide Analytical Manual (PAM)Vol. I (section 102)
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